Energy Consumption and Colour Characteristics of Nettle Leaves during Microwave, Vacuum and Convective Drying (Ilknur Alibas)

background image

Biosystems Engineering (2007) 96 (4), 495–502
doi:

10.1016/j.biosystemseng.2006.12.011

PH—Postharvest Technology

Energy Consumption and Colour Characteristics of Nettle Leaves during

Microwave, Vacuum and Convective Drying

Ilknur Alibas

Faculty of Agriculture, Department of Agricultural Machinery, Uludag University, 16059 Bursa, Turkey; e-mail:

ialibas@uludag.edu.tr

(Received 27 March 2005; accepted in revised form 15 December 2006; published online 5 February 2007)

Nettle leaves (Urtica dioica L.) were dried from an initial moisture content of 441 to 01 (dry basis) by
involving microwave, convective and vacuum drying, respectively. Energy consumption and colour
parameters for the nettle leaves were compared at these different drying conditions. In particular, the
experiments were carried out at four different microwave power levels (500, 650, 750 and 850 W) and air
temperatures (50, 75, 100 and 125 1C) to investigate the effect of these factors on the microwave and
convective drying, respectively. Instead, under vacuum drying conditions both the influence of vacuum (20
and 50 mm [Hg]) and drying temperature (50 and 75 1C) were considered. Drying periods ranged from 4 to 6,
30 to 120 and 35 to 65 min for microwave, convective and vacuum drying, respectively. The semi-empirical
Page’s equation was able to reproduce the experimental drying curves at all operating conditions under
microwave, convective and vacuum drying. The optimum method with respect to the drying period, colour
and energy consumption was the microwave drying at 850 W.

r

2007 IAgrE. All rights reserved

Published by Elsevier Ltd

1. Introduction

Stinging nettle Urtica dioica L. belongs to the family

of Urticaceae. In the past few years, nettle has been
noted as a healing plant because of its considerable
effects on human health both in Turkey and in the other
countries all over the world (

Akgul, 1993

). It is

considered to be a nutritive food. Nettle leaf has a long
history as an herbal remedy and nutritious addition to
the diet. The seeds and leaves of nettle contain minerals
(especially iron), vitamin C, pro-vitamin A (

Allardice,

1993

), amino acids (

Martinez-Para, et al., 1980b

),

ascorbic acid (

Martinez-Para & Torija-Isasa, 1980

), rare

carbohydrates (

Martinez-Para et al., 1980a

), and several

mineral elements (

Weiss, 1988

). It is also known that

nettle has anti-oxidant, antimicrobial, anti-ulcer and
analgesic properties (

Gulcin et al., 2004

). Shoots of

nettle cooked as a potherb are added to soups and can
also be dried for winter use (

Facciola & Cornucopia,

1990

). Although the plants are used principally in

pottage, a tea made from the leaves has traditionally
been drunk (

Chevallier, 1996

).

Nettle is a vegetable which rapidly perishes after

harvest and which is currently consumed only in season.
Drying is the one of the storage methods, which has the
capability of extending the consumption period of
nettles, yet maintaining its nutrition content. Drying is
the process of removing the moisture in the product up
to certain threshold value by evaporation. In this way,
the product can be stored for a long period, since the
activities of the micro-organisms, enzymes or ferments
in the material are suppressed (

Alibas-Ozkan et al.,

2005

).

Different drying methods are used in the drying of

fruits and vegetables. Such as worsening of the taste,
colour and nutritional content of the product, decline in
the density and water absorbance capacity, as well as
shifting of the solutes from the internal part of the
drying material to the surface (

Bouraout et al., 1994

;

Yongsawatdigul & Gunesekaran, 1996

;

Feng & Tang,

ARTICLE IN PRESS

1537-5110/$32.00

495

r

2007 IAgrE. All rights reserved

Published by Elsevier Ltd

background image

1998

;

Lin et al., 1998

;

Drouzas et al., 1999

;

Maskan,

2000, 2001

).

The use of microwave rays in the drying of

agricultural products such as grains (

Adu & Otten,

1996

;

Walde et al., 2002

), vegetables (

Litvin et al., 1998

;

Lin et al., 1998

;

Alibas, 2006

;

Alibas-Ozkan et al., 2005

)

and fruits (

Tulasidas et al., 1997

;

Funebo & Ohlsson,

1998

;

Kadlec et al., 2001

) has become widespread

because it minimises the decline in food quality and
provides a rapid and an effective head distribution in the
material (

Dı´az et al., 2003

), which leads to energy

savings (

Feng, 2002

). Microwave drying creates an effect

for moisture transfer, leading to a water vapour pressure
gradient between the bulk and the surface of the
material, as in the convectional drying methods (

Mas-

kan, 2001

).

Microwave drying creates an effect for moisture

transfer, leading to a water vapour pressure gradient
between the bulk and the surface of the material, as in
the conventional drying methods (

Maskan, 2001

).

Microwave energy applications in the drying of vege-
tables have several advantages including the shortening
of drying time, a homogenous energy distribution on the
material and, formation of suitable dry product
characteristics due to the increase in temperature in
the centre of the material. Among the other benefits of
using microwave drying are inhibition of high surface
temperatures, continuation of the product respiration,
lowered product temperatures when combined with
vacuum drying, reduction in the loss of water-soluble
components and energy savings (

Torringa et al., 2001

).

Vacuum drying is a drying technique which is used for

drying of various products, retaining colour and vitamin
content (

Methakhup et al., 2005

). Vacuum enhances the

mass transfer because of an increased pressure gradient
between the inside and outside of the sample to dry and
maintains a low temperature level essential for thermo-
labile products (

Pere & Rodier, 2002

). Better product

quality with respect to traits such as taste, flavour and
rehydration can be retained via high-degree vacuum
treatment (

Drouzas & Schubert, 1996

). The key benefits

of vacuum drying include lower process temperatures,
less energy usage and hence greater energy efficiency,
improved drying rates, and in some cases, less shrinkage
of the product (

Montgomery et al., 1997

). Vacuum

drying has been successfully applied to many fruits and
vegetables and other heat-sensitive foods. Vacuum dried
materials are characterised by better quality retention of
nutrients and volatile aroma. However, the cost of the
process is high (

Tsami et al., 1998

).

The objectives of this study were to: (i) evaluate the

efficacy of microwave, convective and vacuum drying
technique for nettle leaves; (ii) compare the measured
findings obtained during the drying of nettle with the

predicted values obtained with Page’s thin-layer drying
semi-empirical equation; (iii) determine the changes in
the colour values of the product after drying; and (iv)
determine the optimum drying method for the drying of
nettle, with respect to energy consumption, colour and
drying period.

2. Materials and methods

2.1. Drying experiments

The leaves used in the drying experiments were 25

(

7003) g in weight and were selected from healthy

plants of fresh nettle (Urtica dioica L.) provided from
Karacabey county of Bursa. All the samples were stored
at the temperature of 4

705 1C before being dried.

Fresh chard leaves were pre-treated in chamber of

steamy cooker (Raks Buharlim, Manisa, Turkey) before
drying to reduce enzymatic changes. In order to prevent
colour changes, the cooker was set to produce 100 1C
steam and the chard leaves were exposed to steam for
30 s.

Microwave and convective drying treatment was

performed in a domestic digital combine oven (Arcelik
MD 592, Turkey) with technical features of 230 V,
50 Hz and 2900 W. Microwave energy is capable of
polarising substances. The microwave oven has the
capability of operating at eight different microwave
stages, being 90, 160, 350, 500, 650, 750, 850 and
1000 W. The convective oven has the capability of
operating at nine different temperature stages, being 50,
75, 100, 125, 150, 175, 200, 225 and 250 1C at 1 m/s air
velocity. The area on which microwave and convective
drying is carried out was 327 mm by 370 mm by 207 mm
in size, and consisted of a rotating glass plate with
280 mm diameter at the base of the oven. Glass plate
rotates for 5 min

1

and the direction of 3601 rotation

can be changed by pressing the on/off button. Time
adjustment is done with the aid of a digital clock located
on the oven. The drying temperature of convective oven
can be reached after every weight measured within 5 s.

Vacuum drying treatment was performed in a

laboratory-type vacuum oven (Nuve EV 0180, Turkey)
with technical features of 220 V, 50 Hz, 35 A and
800 W. The temperature of vacuum oven has a
sensitivity of 1 1C, with a maximum temperature of
250 1C. The area on which vacuum drying is carried out
was 300 mm by 200 mm by 250 mm in size. An
analogous vacuum-meter which indicates the vacuum
value in terms of mm [Hg] exists on the vacuum oven.
Time adjustment is done with the aid of a program-
mable clock located on the oven.

ARTICLE IN PRESS

I. ALIBAS

496

background image

Drying experiments were conducted using three

different drying methods, namely, microwave, convec-
tive and vacuum drying. Three different experimental
designs were performed for each method. Microwave
drying trial was carried out at four different microwave
generation powers being 850, 750, 650 and 500 W.
Convective drying trial was carried out at four different
temperatures being 50, 75, 100 and 125 1C. Four
different vacuum-temperature combinations were ob-
tained in vacuum trials by combining two different
vacuum levels i.e., 20 and 50 mm [Hg] and two different
temperature regimes at 50 and 75 1C, and the trials were
realised under the combinations of 50 1C–20 mm [Hg],
50 1C–50 mm [Hg], 75 1C–20 mm [Hg] and 75 1C–50 mm
[Hg]. A laboratory type greasy vacuum pump (Carpa-
nelli MMDE80B4, Italy) was used in the vacuum drying
with operating conditions were 220/240 V, 50/60 Hz
and 51/48 A. The vacuum pump is increased the least
vacuum value within 20 s.

All experiments were conducted at each drying

technique and the values obtained from these trials
were averaged and the drying parameters were deter-
mined. Dried nettle leaves which were being dried were
removed from the oven periodically (every 30 s for
microwave drying and every 5 min for vacuum and
convective drying) during the drying period, and the
moisture loss was determined by weighing the plate
using digital balance (Sartorious EX 2000A, Germany)
with 001 g precision (

Soysal, 2004

;

Alibas, 2006

). All

weighing processes were completed in 10 s during the
drying process. Energy consumption of microwave,
convective and vacuum oven with together vacuum
pump was determined using a digital electric counter
(Kaan, Type 101, Turkey) with 001 kW h precision.
Drying process continued until the moisture content of
nettle fell down to 01

70005 on dry basis.

2.2. Data analysis and empirical drying model

The following common semi-empirical Page’s equa-

tion [Eqn (1)] was used to describe the thin-layer drying
kinetics of nettle leaves (

Soysal, 2004

;

Alibas, 2006

):

M

R

¼

X X

e

X

0

X

e

¼

expððktÞ

n

Þ

,

(1)

where: M

R

is the moisture content ratio; X is the

moisture content at any drying time dry basis (db); X

e

is

the equilibrium moisture content % db; X

o

is the initial

moisture content in % db; t is the drying time in min; k
is the drying constant in min

1

; and n is the dimension-

less exponent.

2.3. Colour parameters

Leaf colour was determined by two readings on the

two different symmetrical faces of the leaf in each
replicate, using a Minolta CR 300 colorimeter (Konica-
Minolta, Osaka, Japan), calibrated with a white
standard

tile.

The

colour

brightness

coordinate

L measures the whiteness value of a colour and ranges
from black at 0 to white at 100. The chromaticity
coordinate a measures red when positive and green
when

negative,

and

the

chromaticity

coordinate

b measures yellow when positive and blue when
negative. Also, the chroma C [Eqn (2)] and hue angle
a [Eqn (3)] were calculated from the values for L, a, b
and used to describe the colour change during drying
(

Soysal, 2004

):

C ¼

ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi

a

2

þ

b

2

p

(2)

a ¼ tan

1

ð

b=aÞ

(3)

2.4. Data analysis

The research was conducted using randomised plots

factorial experimental design. Determination of the
investigated components was carried out in three
replicates. Mean differences were tested for signifi-
cance by using an least significant difference (LSD)
(MSTATC) test at 1% level of significance.

Non-linear regression analysis was performed using

NLREG (NLREG version 63) to estimate the para-
meters k and n of semi-empirical Page’s equation [Eqn
(1)]. Regression results include the coefficients for the
equation and coefficient of determination R

2

.

3. Results and discussion

3.1. Drying curves

Moisture–time diagram of nettle along the drying

period on dry basis is given in

Figs 1–3

for microwave,

convective and vacuum drying, respectively.

A reduction in drying time occurred with increasing

the microwave power level. The time required for the
lowering of moisture content of nettle leaves to 01 from
441 on dry basis varied between 4 and 6 min depending
on the microwave power level. A marked decline was
noted in the drying period of leaves with the increasing
microwave power level (

Prabhanjan et al., 1995

;

Drouzas & Schubert, 1996

;

Funebo & Ohlsson, 1998

;

Soysal, 2004

). The required time for microwave drying

ARTICLE IN PRESS

ENERGY CONSUMPTION AND COLOUR CHARACTERISTICS OF NETTLE LEAVES

497

background image

at 500 W was 15 times longer than that at 850 W. The
drying time reduced by 30 and 15 times in the drying
treatment realised at 50 and 75 1C temperatures and at 1
m/s air velocity compared with the drying treatment
realised at 850 W microwave powers. The moisture
content of the material was very high during the initial
phase of the drying which resulted in a higher
absorption of microwave power and higher drying rates
due to the higher moisture diffusion. As the drying
progressed, the loss of moisture in the product caused a
decrease in the absorption of microwave power and
resulted in a fall in the drying rate. Higher drying rates
were obtained at higher microwave output powers.
Thus, the microwave output power had a crucial effect
on the drying rate (

Soysal, 2004

).

The convective drying process which reduced the

nettle leaves moisture contents from 441 db to moisture
content of 010 db took 30–120 min, depending on the
applied temperature. As the temperature was increased,
the drying time of leaves was significantly reduced
probability (P

o001) (

Demir et al., 2004

;

Mwithiga &

Olwal, 2005

;

Menges & Ertekin, 2005

). By working at

125 1C instead of 50 1C, the drying time up to the
moisture content of 010 db could be shortened by 75%.

A marked decline was observed in the drying period

of nettle leaves with the increasing temperature level and
decreasing vacuum level (

Methakhup et al., 2005

).

Drying time at 50 1C temperature was found as 55 and
65 min for 20 and 50 mm [Hg], respectively, and at 75 1C,
it was found as 35 and 45 min for 20 and 50 mm [Hg]
vacuum values, respectively. Increase in temperature
level in vacuum drying had an important effect on the
reduction of drying time. The extent of drying realised at
50 1C temperature and 50 mm [Hg] vacuum value with
the longest drying period was 186 times higher
compared with the drying process realised at 75 1C and
20 mm [Hg], with the shortest drying period. When the
drying process realised at 50 1C temperature and 1m/s
air velocity without vacuum effect was compared with
the drying processes at 50 1C temperature and with 20
and 50 mm [Hg] vacuum values, the drying period was
shortened by 218 and 185 times, respectively, com-
pared with the drying without vacuum effect. Similarly,
when the drying applications realised at 75 1C with 20
and 50 mm [Hg] vacuum values were compared with
drying process without vacuum at 75 1C and 1m/s air
velocity, the drying period was reduced by 171 and 133
times, respectively, under vacuum.

ARTICLE IN PRESS

0

1

2

3

4

5

0

10

20

30

40

50

60

70

80

90 100 110 120

Convective drying time, min

M

o

isture content,

db

Fig. 2. The convective drying curve of nettle leaves on dry basis;
comparing experimental curve with the predicted one (-) through
semi-empirical Page’s equation [Eqn (1)] for nettle leaves at
various temperatures; K, 125 1C; m, 100 1C; &, 75 1C;—,

50 1C

0

1

2

3

4

5

0

1

2

3

4

5

Microwave drying time, min

Moisture content, db

Fig. 1. The microwave drying curve of nettle leaves on dry basis;
comparing experimental curve with the predicted one (-) through
semi-empirical Page’s equation [Eqn (1)] for nettle leaves at
various microwave levels; K, 850 W; m, 750 W; &, 650 W;—,

500 W

0

1

2

3

4

5

0

10

20

30

40

50

60

70

Vacuum drying time, min

Moisture content, db

Fig. 3. The vacuum drying curve of nettle leaves on dry basis;
comparing experimental curve with the predicted one (-)
through semi-empirical Page’s equation [Eqn (1)] for nettle
leaves at various vacuum and temperature combinations; K,
75 1C and 20 mm [Hg]; m, 75 1C and 50 mm [Hg]; &, 50 1C

and 20 mm [Hg];—, 50 1C and 50 mm [Hg]

I. ALIBAS

498

background image

During the drying of 50 g nettle leaves at three

different drying methods, a total of 3987 g of weight
loss occurred from each drying sample.

3.2. Energy consumption

The energy consumption values obtained during

microwave, convective and vacuum drying of nettle
leaves are given

Fig. 4

. When the three drying methods

were compared with respect to energy consumption
values, it was noted that the lowest energy consumption
occurred in microwave drying method and this was
followed by convective- and vacuum- drying methods.
The best result with regard to energy consumption was
obtained from 850 W microwave levels among all drying
methods.

Energy

consumption

at

this

level

was

006 kW h. The highest value in all drying methods
regarding energy consumption was noted in vacuum
drying process consisting of 50 1C temperature and
50 mm [Hg] vacuuming rate, with 081 kW h. There was
a 135—fold difference between the highest (50 1C-
50 mm [Hg]) and the lowest (850 W) energy consump-
tion values.

3.3. Modelling drying data

The parameters k and n of a semi-empirical Page’s

thin layer drying equation [Eqn (1)] for a given
microwave, convective and vacuum drying condition
were estimated using non-linear regression technique
(

Table 1

) and the fitness is illustrated in

Figs 1–3

,

respectively.

The model gave an excellent fit for all the experi-

mental data points with values for the coefficient of
determination of greater than 09982 at 850 W in
microwave drying, 09994 at 75 1C in convective drying
and 09976 (75 1C–20 mm [Hg]) in vacuum drying. It is
determined that the value of the drying constant k
increased with the increase in microwave power. This
data points out that following the increase in microwave
output power, drying curve becomes steeper, indicating
faster drying of the product. As a result, measured
moisture ratio values and predicted moisture ratio
values were found similar to each other (

Soysal, 2004

;

Alibas-Ozkan et al., 2005

). The drying constant k values

increased with the increasing temperature at all tem-
perature values but 75 1C (

Mwithiga & Olwal, 2005

).

The best coefficient of determination at 50 1C was 09999
at convective drying. The vacuum drying level estab-
lished by combining 50 1C temperature and 20 mm [Hg]
vacuuming rate gave the best result (09999) with respect
to coefficients of determination.

ARTICLE IN PRESS

0

0.8

0.6

0.4

0.2

1

50

°

C, 1 m/s

75

°

C, 1 m/s

100

°

C, 1 m/s

125

°

C, 1 m/s

20 mm[Hg], 75

°

C

20 mm[Hg], 50

°

C

50 mm[Hg], 75

°

C

50 mm[Hg], 50

°

C

500 W

650 W

750 W

850 W

Con

v

ecti

ve

V

acuum

Microw

ave

Energy consumption, kWh

Fig. 4. Energy consumption during the drying of nettle leaves at

three different drying methods

Table 1

Non-linear regression analysis results of semi-empirical Page’s
equation [Eqn (1)] for microwave, vacuum and convective drying
of nettle (

Urtica diocia L.) leaves; k, drying rate constant, min

1

;

n, exponent; SEE, standard error of estimate; R

2

, coefficient of

determination

Drying method

k

(NS)

n

SEE(

7)

(NS)

R

2(NS)

Microwave drying
850 W

01865

20276

001603

09982

750 W

01472

20911

001219

09990

650 W

01171

20335

001185

09990

500 W

00925

19988

001291

09988

Vacuum drying
75 1C–20 mm [Hg]

00373

12348

001721

09976

75 1C–50 mm [Hg]

00345

12155

001148

09989

50 1C–20 mm [Hg]

00368

11492

000396

09999

50 1C–50 mm [Hg]

00354

11302

000665

09996

Convective drying
50 1C

00697

11383

000841

09995

75 1C

00483

11520

000633

09997

100 1C

00251

12006

000826

09994

125 1C

00261

10446

000348

09999

Column mean values with different superscripts are significantly
different.

Probability Po001,

NS

not significant.

ENERGY CONSUMPTION AND COLOUR CHARACTERISTICS OF NETTLE LEAVES

499

background image

3.4. Colour parameters

The colour parameters (L, a, b) formed in microwave,

convective and vacuum drying of nettle leaves are
compared in

Table 2

.

The colour criteria obtained as a result of microwave

(500, 650, 750 and 850 W), convective (50, 75, 100 and
125 1C) and vacuum (50 1C–50 mm [Hg], 50 1C–20 mm
[Hg], 75 1C–50 mm [Hg] and 75 1C–20 mm [Hg]) drying
the nettle leaves, and the colour criteria obtained from
the fresh nettle leaves. An important loss was noted in
the values for L, a, and b of dried nettle leaves when
compared with fresh leaves.

The highest loss in brightness was determined in

500 W microwave power levels in microwave drying. A
higher value was obtained at 850 W in comparison with
the other power levels. Values similar to the results
obtained for L values were obtained with a, b values.
The colour values nearest to those of fresh nettle leaves
were reached in the drying applications made by using
850 W microwave powers. Similar results were obtained
by

Chua and Chou (2005)

. They examined the colour

change in carrot as influenced by 100, 300 and 500 W
microwave powers and determined the slightest colour
change in 500 W microwave output powers. According
to

Schiffmann (1995)

, high moisture bio-products

undergoing microwave drying have the advantage.
Microwave drying removes the moisture on the surface
by converting it to water vapour; it results in drying

without causing surface overheating phenomena. There-
fore, in terms of surface colour degradation, preserva-
tion of the product colour was good. It is estimated that
the products are subjected to high temperature with the
increasing power levels during microwave drying (

Chua

& Chou, 2005

). For this reason, the product colour is

also adversely affected, since the microwave drying
period is longer in the drying process realized at very
low microwave powers, and thus the product is
subjected to heat for a longer time (

Sumnu et al.,

2005

). Also, in this study, the low values measured in L,

a, and b colour criteria measured at 500 W microwave
power are supported by the results in the previous
research given above.

The greatest loss in brightness was determined at 125 1C

temperature value in convective drying. Higher values
were obtained at 50 1C temperature compared with the
other treatments. Similar values were obtained also for a,
and b values. Colour values nearest to those of fresh nettle
leaves were reached with drying at 50 1C temperature.

Doymaz and Pala (2002)

examined the colour change in

red pepper at 50 and 60 1C; and determined the slightest
colour change at 50 1C temperature.

Demir et al. (2004)

dried bay leaves at 40, 50 and 60 1C and obtained the best
colour value at 50 1C. The products are subjected to high
temperatures with the increasing temperature during
convective drying. Therefore, the product colour is
adversely affected by convective drying applications
realised at high temperatures.

ARTICLE IN PRESS

Table 2

Comparison between microwave, vacuum and convective drying methods for colour parameters during nettle leaves drying
(

L, brightness (+100)/ darkness (+0); a, redness (+50)/greenness (50) coordinate; b, yellowness (+50)/blueness (50)

coordinate;

C, chroma; a1, hue angle)

Drying method

Colour parameters

L

a

b

C

a1

Fresh

2764

a

(

70330)

686

a

(

70176)

967

a

(

70146)

1185

a

(

70216)

12535

ab

(

7037)

Microwave drying
850 W

2693

ab

(

70209)

665

a

(

70116)

919

ab

(

70180)

1134

ab

(

70210)

12588

a

(

7023)

750 W

2650

bcd

(

70227)

641

ab

(

70169)

898

bc

(

70068)

1103

bc

(

70153)

12553

a

(

7051)

650 W

2612

bcde

(

70087)

613

bc

(

70069)

874

bcd

(

70099)

1068

bcd

(

70120)

12507

ab

(

7006)

500 W

2571

de

(

70207)

586

cd

(

70144)

833

de

(

70197)

1019

de

(

70244)

12514

ab

(

7003)

Vacuum drying
75 1C–20 mm [Hg]

2659

bc

(

70217)

646

ab

(

70154)

899

bc

(

70076)

1107

bc

(

70152)

12570

a

(

7042)

75 1C–50 mm [Hg]

2606

cde

(

70030)

610

bc

(

70029)

866

cd

(

70032)

1059

cd

(

70043)

12515

ab

(

7003)

50 1C–20 mm [Hg]

2569

de

(

70155)

584

cd

(

70092)

832

de

(

70142)

1017

de

(

70170)

12506

ab

(

7003)

50 1C–50 mm [Hg]

2485

fg

(

70147)

546

de

(

70115)

783

ef

(

70104)

954

ef

(

70151)

12489

ab

(

7022)

Convective drying
50 1C

2544

ef

(

70121)

566

cd

(

70093)

808

e

(

70127)

986

e

(

70158)

12504

ab

(

7004)

75 1C

2418

g

(

70072)

502

e

(

70047)

745

f

(

70049)

899

f

(

70067)

12398

b

(

7008)

100 1C

2219

h

(

70199)

323

f

(

70177)

610

g

(

70139)

691

g

(

70205)

11788

c

(

7077)

125 1C

1963

i

(

70383)

200

g

(

70139)

508

h

(

70194)

556

h

(

70230)

11139

d

(

7067)

Probability Po001 Column mean values with different superscripts are significantly different.

I. ALIBAS

500

background image

In vacuum drying, the greatest loss in brightness was

determined at 50 1C temperature and 50 mm [Hg]
vacuum combinations. Values nearest to the colour
values (L, a, and b) of fresh nettle leaves were obtained
with the combinations of 75 1C–20 mm [Hg] and
75 1C–50 mm [Hg].

In all drying methods, colour values closest to those

of fresh nettle leaves were obtained in microwave drying.
The brightness L value most approximate to those of
fresh nettle leaves was determined in 850 W microwave
power levels, while the most distant brightness L value
was found at 125 1C temperature.

4. Conclusion

The effects of three different drying methods on the

drying of nettle leaves were evaluated based on the
drying parameters such as the drying time, the moisture
content on dry basis, the drying rate, energy consump-
tion and colour criteria. The microwave drying period
was completed between 45 and 6 min at the microwave
powers between 750 and 500 W, while the energy
consumption was constant (007 kW h). The energy
consumption at 850 W microwave levels with the short-
est drying period (4 min) was determined as 006 kW h.
The most suitable methods after microwave drying
method with respect to energy consumption are
convective-drying and vacuum-drying methods, in
decreasing suitability order. Drying period lasted for
30–120 min in convective-drying method, depending on
temperature level (125–50 1C). The drying period in
vacuum drying method ranged from 35 to 65 min,
depending

on

vacuum-temperature

combination

(50 1C–50 mm [Hg] and 75 1C–20 mm [Hg]). Results
closest to those of fresh products with respect to colour
criteria were obtained from microwave drying method,
and this was followed by vacuum and convective drying
methods, in order. The best values of colour criteria,
drying time, energy consumption and drying rate were
obtained at 850 W microwave power levels.

References

Adu B; Otten L (1996). Diffusion characteristics of white beans

during microwave drying. Journal of Agricultural Engineer-
ing Research, 64(1), 61–69

Akgul A (1993) Spices Science and Technology. Association

Food Technology, Publ. No. 15. Ankara, Turkey

Alibas I (2006). Characteristics of chard leaves during

microwave, convective, and combined microwave-convec-
tive drying. Drying Technology, 24, 1425–1435

Alibas-Ozkan I; Akbudak B; Akbudak N (2005). Microwave

drying characteristics of spinach. Journal of Food Engineer-
ing, 78(2), 577–583

Allardice P (1993). A–Z of Companion Planting. Cassell

Publishers Ltd, London

Bouraout M; Richard R; Durance T (1994). Microwave and

convective drying of potato slides. Journal of Food Process
Engineering, 17, 353–363

Chevallier A (1996). The Encyclopedia of Medicinal Plants.

Dorling Kindersley, London

Chua J K; Chou K S (2005). A comparative study between

intermittent microwave and infrared drying of bioproducts.
International Journal of Food Science and Technology, 40,
23–39

Demir V; Gunhan T; Yagcioglu A K; Degirmencioglu A (2004).

Mathematical modelling and the determination of some
quality parameters of air-dried bay leaves. Biosystems
Engineering, 88, 325–335

Dı´az G R; Martı´nez-Monzo´ J; Fito P; Chiralt A (2003).

Modelling of dehydration-rehydration of orange slices in
combined microwave/air drying. Innovative Food Science &
Emerging Technologies, 4, 203–209

Doymaz I; Pala M (2002). Hot-air drying characteristics of red

pepper. Journal of Food Engineering, 55, 331–335

Drouzas A E; Schubert H (1996). Microwave application in

vacuum drying of fruits. Journal of Food Engineering, 28,
203–209

Drouzas A E; Tsami E; Saravacos G D (1999). Microwave/

vacuum drying of model fruit gels. Journal of Food
Engineering, 39, 117–122

Facciola S; Cornucopia A (1990). Source Book of Edible

Plants. Kampong Publications, Vista

Feng H (2002). Analysis of microwave assisted fluidized-bed

drying of particulate product with a simplified heat and
mass transfer model. International Communications in Heat
and Mass Transfer, 29, 1021–1028

Feng H; Tang J (1998). Microwave finish drying of diced apple

slices in a spouted bed. Journal of Food Science, 63,
679–683

Funebo T; Ohlsson T (1998). Microwave-assisted air dehydra-

tion of apple and mushroom. Journal of Food Engineering,
38, 353–367

Gulcin I; Kufrevioglu O I; Oktay M; Buyukokuroglu M E

(2004). Antioxidant, antimicrobial, antiulcer and analgesic
activities of nettle (Urtica dioica L). Journal of Ethnophar-
macology,, 90(2–3), 205–215

Kadlec P; Rubecova A; Hinkova A; Kaasova J; Bubnik Z; Pour

V (2001). Processing of yellow pea by germination,
microwave treatment and drying. Innovative Food Science
and Emerging Technologies, 2, 133–137

Lin T M; Durance T D; Seaman C H (1998). Characterization

of vacuum microwave air and freeze dried carrot slices.
Food Research International, 4, 111–117

Litvin S; Mannheim C H; Miltz J (1998). Dehydration of

carrots by a combination of freeze drying, microwave
heating and air or vacuum drying. Journal of Food
Engineering, 36, 103–111

Martı´nez-Para M C; Fidanza F; Torija-Isasa M E (1980a). La

ortiga en la alimentacio´n [English tradition IV] Fibra
alimentaria. Anales de Bromatologı´a, 32, 109–118

Martı´nez-Para M C; Fidanza F; Torija-Isasa M E (1980b). La

ortiga en la alimentacio´n [English tradition V] Estudio de la
proteı´na. Anales de Bromatologı´a, 32, 309–314

Martı´nez-Para M C; Torija-Isasa M E (1980). La ortiga en la

alimentacio´n [English tradition III] Ascorbic acid. Anales de
Bromatologı´a, 32, 295–298

ARTICLE IN PRESS

ENERGY CONSUMPTION AND COLOUR CHARACTERISTICS OF NETTLE LEAVES

501

background image

Maskan M (2000). Microwave/air and microwave finish drying

of banana. Journal of Food Engineering, 44, 71–78

Maskan M (2001). Drying, shrinkage and rehydration

characteristics of kiwifruits during hot air and microwave
drying. Journal of Food Engineering, 48, 177–182

Menges O H; Ertekin C (2005). Mathematical modelling of

thin layer drying of Golden apples. Journal of Food
Engineering, 77(1), 119–125

Methakhup S; Chiewchan N; Devahastin S (2005). Effects of

drying methods and conditions on drying kinetics and
quality of Indian gooseberry flake. LWT—Food Science
and Technology, 38(6), 579–587

Montgomery S W; Goldschmidt V W; Franchek M A (1997).

Vacuum assisted drying of hydrophilic plates: static drying
experiments. International Journal of Heat Mass Transfer,
41, 735–744

Mwithiga G; Olwal J O (2005). The drying kinetics of kale

(Brassica oleracea) in a convective hot air dryer. Journal of
Food Engineering, 71, 373–378

Pere C; Rodier E (2002). Microwave vacuum drying of porous

media: experimental study and qualitative considerations of
internal transfers. Chemical Engineering and Processing, 41,
427–436

Prabhanjan D G; Ramaswamy H S; Raghavan G S V (1995).

Microwave assisted convective air drying of thin layer
carrots. Journal of Food Engineering, 25, 283–293

Schiffmann R F (1995) Microwave and dielectric drying. In:

Handbook of Industrial Drying (Mujumdar A S (ed), pp
345–372. New York, USA

Soysal Y (2004). Microwave drying characteristics of parsley.

Biosystems Engineering, 89, 167–173

Sumnu G; Turabi E; Oztop M (2005). Drying of carrots in

microwave and halogen lamp–microwave combination
ovens. LWT—Food Science and Technology, 38, 549–553

Torringa E; Esveld E; Scheewe I; van den Berg R; Bartels P

(2001). Osmotic dehydration as a pre-treatment before
combined microwave-hot-air drying of mushrooms. Journal
of Food Engineering, 49, 185–191

Tsami E; Krokida M K; Drouzas A E (1998). Effect of drying

method on the sorption characteristics of model fruit
powders. Journal of Food Engineering, 38, 381–392

Tulasidas T N; Ratti C; Raghavan G S V (1997). Modelling of

microwave drying of grapes. Canadian Agricultural En-
gineering, 39(1), 57–67

Walde S G; Balaswamy K; Velu V; Rao D G (2002). Microwave

drying and grinding characteristics of wheat (Triticum
aestivum). Journal of Food Engineering, 55, 271–276

Weiss R F (1988). Herbal Medicine. Beaconseld Publishers,

London

Yongsawatdigul J; Gunasekaran S (1996). Microwave-vacuum

drying of cranberries: part II, quality evaluation. Journal of
Food Processing and Preservation, 20, 145–156

ARTICLE IN PRESS

I. ALIBAS

502


Document Outline


Wyszukiwarka

Podobne podstrony:
Improving nutritional value of dried blueberries combining microwave vacuum, hot air drying and free
The energy consumption and economic costs of different vehicles used in transporting woodchips Włoch
Effective Moisture Diffusivity of Plain Yogurt Undergoing Microwave Vacuum Drying
Experimental study on drying of chilli in a combined Microwave vacuum rotary drum dryer (Weerachai K
Characterization of microwave vacuum drying and hot air drying of mint leaves (Mentha cordifolia Opi
Drying, shrinkage and rehydration characteristics of kiwifruits during hot air and microwave drying
Improved Characterization of Nitromethane, Nitromethane Mixtures, and Shaped Charge Jet
Production and Characterisation of extracts
EFFECTS OF EATING AND NOT EATING ON ENERGY STORES AND BODY WEIGHT
Detection and Molecular Characterization of 9000 Year Old Mycobacterium tuberculosis from a Neolithi
38704314 SM01 Intro Conservation of Information Energy Entropy And Temperature
#1038 Types and Characteristics of Apartments
Mirlin Statistics of energy levels and eigenfunctions in disordered systems (PR326, p259, 2000)(124s
Corrosion behavior and surface characterization of titanium
2001 In vitro fermentation characteristics of native and processed cereal grains and potato
Microwave drying characteristics of potato and the effect of different microwave powers on the dried
Bell locality and the nonlocal character of nature
Drying kinetics and rehydration characteristics of microwave vacuum and convective hot air dried mus
DIN 61400 21 (2002) [Wind turbine generator systems] [Part 21 Measurement and assessment of power qu

więcej podobnych podstron